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1. Study on Synthesis and Electrochemical Performance of PMo-PDDA-GO Composite | |||
Ding Chao ,Gu Dawei,Lu Yi ,Xu Tianye ,Sun Hongshun,Li Jishu, Wang Lei,Shen Linjiang | |||
Chemistry 28 March 2017 | |||
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Abstract:A series of composites containing polyoxometalate (PMo), poly (diallyldimethylammonium chloride) (PDDA), and graphene oxide (GO) with different oxidation degrees were prepared in a two-step self-assembly process. The resulting polyoxometalate-poly (diallyldimethylammonium chloride)-graphene oxide (PPGx, x = 1 to 5) composites and their precursors (PDDA-GOx, x = 1 to 5) were analyzed with AFM, XRD, and FTIR spectroscopy. The self-assembly process was schematically summarized. The interspace distance between GO sheets in PPGx increased when the oxidation degree of GO increased. This increase in interspace distance was accompanied by a rapid decrease in the electrical conductivity of PPGx. At a sufficient high oxidation degree (x > 3), PDDA was completely inserted into the interspace of the laminated structure of the GO sheets in PPGx. The experimental results indicated that PDDA acted as a bridge, increasing electrostatic interaction between PMo anions and the GO sheets and causing many PMo anions to become anchored on the GO sheets. The electrochemical performances of the PPGx composites were greatly enhanced by the immobilization of PMo anions on GO sheets via PDDA, resulting in a much larger specific capacitance and a remarkably enhanced cycling stabilityIn this paper. | |||
TO cite this article:Ding Chao ,Gu Dawei,Lu Yi , et al. Study on Synthesis and Electrochemical Performance of PMo-PDDA-GO Composite[OL].[28 March 2017] http://en.paper.edu.cn/en_releasepaper/content/4723025 |
2. Effect of Drying Time on the Antimony Doped Tin Dioxide Coated Titanium Electrode | |||
WANG Yun-Hai,ZHOU Zhe,LI Guo,CHEN Qing-Yun | |||
Chemistry 06 January 2013 | |||
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Abstract:The antimony doped tin dioxide coated titanium electrodes were prepared by dip-coating pyrolysis method with different drying time. The effect of drying time on the electrode activity, morphology, crystallinity and composition were discussed. The results indicated that electrode prepared by drying 10 minutes had higher activity towards phenol degradation than those prepared by drying 0 or 30 minutes. The relation between the activity and oxygen vacancies concentration was discussed. The TG-DTA analysis was used to monitor the reactions occurred during the electrode preparation. The results showed that there were three endothermic or exothermal peaks and the possible reactions were discussed. | |||
TO cite this article:WANG Yun-Hai,ZHOU Zhe,LI Guo, et al. Effect of Drying Time on the Antimony Doped Tin Dioxide Coated Titanium Electrode[OL].[ 6 January 2013] http://en.paper.edu.cn/en_releasepaper/content/4500284 |
3. Influence of Fluoride-doped Tin Oxide Interlayer on Ni-Sb-SnO2/Ti Electrodes | |||
LI Guo,WANG Yun-Hai,CHEN Qing-Yun | |||
Chemistry 11 December 2012 | |||
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Abstract:In the present work, fluoride doped tin oxide (FTO) as an interlayer was introduced into nickel and antimony co-doped tin dioxide (NATO) coated titanium electrodes to investigate the influence of FTO interlayer on the structural properties and lifetime performance of the electrodes. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) techniques were used to characterize the morphology and crystal structure of the electrodes with or without FTO interlayer. The electrode surface became smoother with FTO interlayer introduced while the crystallite size reduced. Electrochemical impedance spectroscopy (EIS) was also adopted to analyze the electrodes' electrochemical behavior. With FTO interlayer introduced, the formation of titanium dioxide insulating layer on the titanium substrate was significantly retarded during the anodic process. The accelerated lifetime tests presented that the lifetime of the electrodes with proper FTO interlayer was 6 times longer than that without FTO interlayer. The mechanisms for the electrodes' lifetime enhancement with FTO interlayer were discussed. | |||
TO cite this article:LI Guo,WANG Yun-Hai,CHEN Qing-Yun. Influence of Fluoride-doped Tin Oxide Interlayer on Ni-Sb-SnO2/Ti Electrodes[OL].[11 December 2012] http://en.paper.edu.cn/en_releasepaper/content/4500527 |
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