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1. Energetic Properties and Stabilities of Iron and Zinc Complexes of N,N-bis(1(2)H-tetrazol-5-yl)amine | |||
DONG Linlin,HE Ling,TAO Guohong | |||
Chemistry 07 October 2013 | |||
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Abstract:The iron (2) and zinc (3) complexes based on N,N-bis(1(2)H-tetrazol-5-yl)amine (H2BTA, 1) were prepared. Complexes 2 and 3 were characterized by differential scanning calorimeter (DSC) and thermogravimetric analysis (TGA) to estimate their thermal stabilities. These complexes are thermal stable with first loss of the coordinated water and then decomposed at higher temperature (330-360 C). Their sensitivities toward impact along with friction were tested by BAM standards. Complexes 2 and 3 are insensitive to neither impact (>40 J) nor friction (>360 N), which can be classed as insensitive energetic materials. Their standard heats of formation were investigated based on the heats of combustion performed by bomb calorimetry. Complexes 2 and 3 are of interest as potential energetic materials with high nitrogen content (~60%), high heats of formation, high oxygen balance, high thermal stability as well as low sensitivity to impact and friction. | |||
TO cite this article:DONG Linlin,HE Ling,TAO Guohong. Energetic Properties and Stabilities of Iron and Zinc Complexes of N,N-bis(1(2)H-tetrazol-5-yl)amine[OL].[ 7 October 2013] http://en.paper.edu.cn/en_releasepaper/content/4563053 |
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