Confined Synthesis of Silicalite-1 Hollow Spheres with a Lamellar Shell

CHEN Huiyong

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Confined Synthesis of Silicalite-1 Hollow Spheres with a Lamellar Shell

CHEN Huiyong * #

School of Chemical Engineering, Northwest University, Xi'an, 710069

*Correspondence author

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Funding: National Natural Science Foundation of China （No.No. 21306151）, Natural Science Foundation of Shaanxi Province of China（No.No. 2014JQ2054, No. 2013JK0694）, Specialized Research Fund for the Doctoral Program of Higher Education of China （No.No. 20136101120008）

Opened online:15 August 2014

Accepted by: none

Citation: CHEN Huiyong.Confined Synthesis of Silicalite-1 Hollow Spheres with a Lamellar Shell[OL]. [15 August 2014] http://en.paper.edu.cn/en_releasepaper/content/4606221

A novel synthesis strategy with integrated using soft/hard templates was proposed for the confined synthesis of silicalite-1 hollow spheres with a lamellar shell. Replicated from macroporous carbon templates and directed by multi-quaternary ammonium surfactants, the silicalite-1 spheres demonstrated unique hollow nanoshell morphology, high crystallinity, and novel hierarchical porosity consisted of hollow macropores, interlamellar mesopores and ordered micropores in zeolites.

Keywords:chemical engineering; hierarchical zeolite; confined synthesis; silicalite-1; hollow sphere; lamellar structure

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