Decarboxylative (4+1) Oxidative Annulation of Malonate Monoesters with 2-Vinylpyridine Derivatives

TANG Shan; GAO Xinlong; LEI Aiwen

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Decarboxylative (4+1) Oxidative Annulation of Malonate Monoesters with 2-Vinylpyridine Derivatives

TANG Shan,GAO Xinlong,LEI Aiwen * #

College of Chemistry and Molecular Sciences, Wuhan University, Wuhan, Hubei, 430072, China.

*Correspondence author

#Submitted by

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Funding: 973 Program （No.2012CB725302）, Research Fund for the Doctoral Program of Higher Education of China（No.20120141130002）, Ministry of Science and Technology of China（No.2012YQ120060）, Hubei Province Natural Science Foundation of China （No.2013CFA081）, National Natural Science Foundation of China（No.21390400, 21520102003, 21272180, 21302148）

Opened online: 8 June 2016

Accepted by: none

Citation: TANG Shan,GAO Xinlong,LEI Aiwen.Decarboxylative (4+1) Oxidative Annulation of Malonate Monoesters with 2-Vinylpyridine Derivatives[OL]. [ 8 June 2016] http://en.paper.edu.cn/en_releasepaper/content/4695660

A novel N-iodosuccinimide mediated decarboxylative (4+1) oxidative annulation between 2-vinylpyridine derivatives and malonate monoesters was developed. It offered a new way to construct indolizines derivatives by utilizing malonate monoesters as C1 unit. Alkyl 2,2-diiodoacetate was found to be the active reaction intermediate during the transformation.

Keywords:Organic chemistry, decarbonylation; indolizine; oxidative annulation

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