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Sponsored by the Center for Science and Technology Development of the Ministry of Education
Supervised by Ministry of Education of the People's Republic of China
A simple co-precipitation technique was successfully used to synthesize fine powders of SnNb2O6 (when Sn2+: Nb5+=1: 2) and Sn2Nb2O7 (when Sn2+: Nb5+=1: 1) phase by calcining precursor at 700 °C. This is a much lower temperature as compared to that prepared by traditional solid-state method (900 °C), as reported for the formation of SnNb2O6 and Sn2Nb2O7. And the average particle sizes of the two phases above are about 80 nm and 50 nm respectively according to the powder X-ray diffraction (XRD) and Transmission electron microscope (TEM) images. The forming processes of the two phases were investigated by XRD and DSC-TG curves. Photocatalytic properties of the powders were investigated by measuring degradation of methyl orange in aqueous solution under light irradiations.